Self assembly directed synthesis of tubular conduction polymer inside th channels of MCM-41

Ali Md Showkat; Kwang-Pill Lee; Anantha Iyengar Gopalan; K Raghava Reddy; Sang-Ho Kim; 최성호

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P-ISSN1225-0163
E-ISSN2288-8985
SCOPUS, ESCI, KCI

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P-ISSN 1225-0163
E-ISSN 2288-8985

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Self assembly directed synthesis of tubular conduction polymer inside th channels of MCM-41

분석과학 / Analytical Science and Technology, (P)1225-0163; (E)2288-8985

2006, v.19 no.3, pp.211-217

Ali Md Showkat (경북대학교)
Kwang-Pill Lee (경북대학교)
Anantha Iyengar Gopalan (경북대학교)
K Raghava Reddy (경북대학교)
Sang-Ho Kim (경북대학교)
최성호 (한남대학교)

Ali, M. S. , Kwang-Pill, L. , Anantha, I. G. , K, R. R. , Sang-Ho, K. , & 최성호. (2006). . , 19(3), 211-217.

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Abstract

Diphenyl amine (DPA) was polymerized inside the channels of the mesoporous silica (MCM-41). MCM-41 (C) and MCM-41 (D) were prepared with cetyltrimethyl ammonium bromide (CTAB) and dodecyltrimethyl ammonium bromide (DTAB), respectively and used as hosts. Initially, the self assembly of DPA inside the pores of MCM-41 was made in β-naphthalene sulfonic acid (NSA) medium and subsequently poly (diphenylamine), PDPA was formed by oxidative polymerization. N2 adsorption-desorption measurements of PDPA loaded MCM-41 (C) and MCM-41 (D) show variations in pore volume and surface area between them. A tubular form of poly (diphenylamine), PDPA was envisaged to form in the pores of MCM-41 and supported by high resolution transmission microscopy. The presence of PDPA inside the channel of MCM-41 was further confirmed by FTIR spectroscopy, thermogravimetric analysis (TGA), X-ray diffraction.

keywords: Mesoporous silica (MCM-41), poly (diphenylamine), self-assembly

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Self assembly directed synthesis of tubular conduction polymer inside th channels of MCM-41

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