- P-ISSN 2233-4203
- E-ISSN 2093-8950
- P-ISSN2233-4203
- E-ISSN2093-8950
- ESCI, SCOPUS, KCI
논문 상세
Home > 논문 상세
A Simple Method for Determining Residual p-arsanilic Acid in Aquatic Products using EDTA-Assisted Solvent Extraction and LC-MRM
Mass Spectrometry Letters / Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950
2023, v.14 no.2, pp.36-41
https://doi.org/10.5478/MSL.2023.14.2.36
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
(College of Pharmacy, Dankook University)
Kwon,
M. K., Shin,
Y. B., Kim,
Y. M., Kim,
J. H., Kim,
J. S., &
Choi,
Y.
S.
(2023). . , 14(2), 36-41, https://doi.org/10.5478/MSL.2023.14.2.36
- 다운로드 수
- 조회수
Abstract
A simple method was developed to determine residual p-arsanilic acid (ASA), an organo-arsenic compound used as a feed additive, in aquatic products (eel, halibut, and shrimp) using EDTA-assisted solvent extraction and LC-MRM. The method was successfully validated in terms of specificity, linearity (coefficient of determination ≥ 0.995), accuracy (recovery or R, 72.72-78.73%), precision (the relative standard deviation of R, 2.08-6.98%), and sensitivity (the lower limit of quantitation, 5 ppb) according to CODEX guidelines (CAC-GL 71-2009). The use of EDTA in the extraction solvent and water with a suitable pH modifier as the reconstitution solvent may be the key factors for successful results. This is the first method that can be used for monitoring residual ASA in aquatic products using LC-MRM and could contribute to establishing a better aquatic product safety management system.
- keywords
- p-arsanilic acid, MRM, EDTA, solvent extraction, halibut, eel, shrimp, aquatic products
- 투고일Received
- 2023-06-16
- 수정일Revised
- 2023-06-23
- 게재확정일Accepted
- 2023-06-25
- 출판일Published
- 2023-06-30
권호 내 다른 논문
- Phytochemical Compounds from the Ethanolic Extract of Gymnema sylvestre, Senna auriculata and Cissus quadrangularis through GC-MS Analysis
- A Simple Method for Determining Residual p-arsanilic Acid in Aquatic Products using EDTA-Assisted Solvent Extraction and LC-MRM
- A Plant Metabolomic Approach to Identify the Difference of the Seeds and Flowers Extracts of Carthamus tinctorius L.
- Investigating the Efficiency of Formic Acid and Hydrochloric Acid in Weak Acid Hydrolysis for Myoglobin
- more
추천 논문
학술지 홈페이지 이용 환경은 크롬 브라우저 사용을 권장합니다.