Improvement of Analytical Method for Determination of Germanium in Plant by Atomic Absorption Spectrometry

Han, Seong-Soo; 한성수; Rim, Yo-Sup; 임요섭; Kim, Il-Kwang; 김일광

오늘 하루 그만보기

P-ISSN1225-0163
E-ISSN2288-8985
SCOPUS, ESCI, KCI

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P-ISSN 1225-0163
E-ISSN 2288-8985

e-Submission

Vol.10, No.3

PubReader Citation

Improvement of Analytical Method for Determination of Germanium in Plant by Atomic Absorption Spectrometry

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985

1997, v.10 no.3, pp.179-186

Han, Seong-Soo
Rim, Yo-Sup
Kim, Il-Kwang

Han, S., Rim, Y., & Kim, I. (1997). Improvement of Analytical Method for Determination of Germanium in Plant by Atomic Absorption Spectrometry. , 10(3), 179-186.

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Abstract

This study was carried out to improve the analytical method for determination of germanium in plants by atomic absorption spectrometry with graphite furnace. For the decomposition of plant samples, the mixed acid of $HNO_3+HClO_4+H_2SO_4$(10 : 4 : 1, v/v) was used. Under this condition, time requirement for the decomposition was 4~5 days and recovery rate was more than 98%. Solution for filling up to constant volume after decomposition was 0.1M acetic acid-sodium acetate. Detection limit for determination of germanium was 0.02 ppm by atomic absorption spectrometry with graphite furnace and argon gas. These results were corresponded with the above-mentioned research projects for improving the determination method of germanium in plants.