Preparation and characterization of fullerene dimer [C120] by trichloroperbenzoic acid oxidation method

오원춘; 정아름; 고원배

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P-ISSN1225-0163
E-ISSN2288-8985
SCOPUS, ESCI, KCI

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P-ISSN 1225-0163
E-ISSN 2288-8985

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Preparation and characterization of fullerene dimer [C120] by trichloroperbenzoic acid oxidation method

분석과학 / Analytical Science and Technology, (P)1225-0163; (E)2288-8985

2007, v.20 no.2, pp.124-130

오원춘 (한서대학교)
정아름 (한서대학교)
고원배 (삼육대학교)

오원춘, 정아름, & 고원배. (2007). . , 20(2), 124-130.

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Abstract

In this study, we present the preparation and characterization of oxidized fullerene and fullerene dimer [$C_{120}$]. From the XRD data, other weak peaks with pristine fullerene [$C_{60}$] peaks were observed in the X-ray diffraction patterns for fullerene dimer [$C_{120}$]. SEM micrographs for the fullerene dimer [$C_{120}$] indicated that practically all the surface state was shown the drastic morphology changes and its outer surface is clearly visible and resulted in clogging and frost-like formation. From the MALDI-TOF mass spectra, the differences in the spectra recorded on two kinds of fullerene are due to the oxidation including chemical bonding and bridging between the $C_{60}$ molecules. We also obtained additional information from FT-IR spectra on functional component on the chemically modified surface of oxidized fullerene and fullerene dimer [$C_{120}$].

keywords: fullerene dimer [<TEX>$C_{120}$</TEX>], XRD, SEM, MALDI-TOF, FT-IR

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Preparation and characterization of fullerene dimer [C120] by trichloroperbenzoic acid oxidation method

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