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  • P-ISSN1225-0163
  • E-ISSN2288-8985
  • SCOPUS, ESCI, KCI

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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

Quantitative analysis of phosphorus by HERETIC-NMR method

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2008, v.21 no.5, pp.438-441



Abstract

We have developed an alternative to the internal chemical reference based on a calibrated reference signal which is not a real NMR line but an electronically produced signal (HERETIC) and determined the phosphorus concentration using this method. The area ratio of HERETIC and sample peaks obtained from the standard samples was used to measure the concentrations of different samples directly. The analysis of phosphorus by this method showed the excellent linear regression coefficient (R2=0.9999) for the concentration range from 20 ppm to 500 ppm with HERETIC peak as reference.

keywords
phosphorus analysis, NMR, HERETIC

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Analytical Science and Technology