Analytical method of New POPs in environmental samples

신선경; 박진수; 강영렬; 이수영; 전진원; 김동훈; 연진모

doi:10.5806/AST.2010.23.2.128

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P-ISSN 1225-0163
E-ISSN 2288-8985

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Vol.23, No.2

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Analytical method of New POPs in environmental samples

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985

2010, v.23 no.2, pp.128-137

https://doi.org/10.5806/AST.2010.23.2.128

& (2010). Analytical method of New POPs in environmental samples. , 23(2), 128-137, https://doi.org/10.5806/AST.2010.23.2.128

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Abstract

The purpose of this study is to set up the analytical method of new persistent organic pollutants (POPs)such as chlordecone, endosulfan, α-HCH, β-HCH, γ-HCH. The analytical methods for these compounds listed as new POPs by the Stockholm Convention need to be newly established. Therefore, we proposed the analytical method for 5 organic chlorinated pesticides (OCPs) and then applied the analytical method to environmental samples. To do this, the pre-treatment such as florisil and activated carbon cleanup process in the Korean official method for classic POPs had been reviewed. All of compounds except chlordecone were pre-treated simultaneously with reviewed cleanup process and detected by GC/MS and HRGC/HRMS respectively. There is a problem that chlordecone could not get a high sensitivity by GC analysis, but in this study GC/MS method was proposed.