Comparison of recovery rates of DNPH-Cartridge sampler in the analysis of odorous carbonyl compounds

홍원필; 임승민; 김기현

doi:10.5806/AST.2010.23.5.446

오늘 하루 그만보기

P-ISSN1225-0163
E-ISSN2288-8985
SCOPUS, ESCI, KCI

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P-ISSN 1225-0163
E-ISSN 2288-8985

e-Submission

Vol.23, No.5

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Comparison of recovery rates of DNPH-Cartridge sampler in the analysis of odorous carbonyl compounds

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985

2010, v.23 no.5, pp.446-456

https://doi.org/10.5806/AST.2010.23.5.446

& (2010). Comparison of recovery rates of DNPH-Cartridge sampler in the analysis of odorous carbonyl compounds. , 23(5), 446-456, https://doi.org/10.5806/AST.2010.23.5.446

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Abstract

In this study, the performance characteristics of DNPH sampling were investigated in the collection and analysis of 5 carbonyl compounds (CC) in air using the cartridge products produced by three different makers. For these experiments, gaseous standards of 5 CCs were prepared to cover 9 concentration levels for each compound (33~2600 nmol). Some cartridge products exhibited relatively high blank values of acetaldehyde (AA) and propionaldehyde (PA). The recovery rates of all three cartridges showed moderate reduction as the molecular weight of CC increased. In addition, when the recovery rate was compared by percent error (%), the most stable patterns were achieved in the intermediate concentration range of 263~1312 nmol (in case of AA). The overall results of our study suggest that the optimal range of recovery for a given concentration range should be considered to obtain the most reliable data for the DNPH cartridge method.