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  • P-ISSN1225-0163
  • E-ISSN2288-8985
  • SCOPUS, ESCI, KCI

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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

Development of the testing method for vinyl chloride monomer (VCM) in polyvinyl chloride(PVC) samples

Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2012, v.25 no.6, pp.395-401
https://doi.org/10.5806/AST.2012.25.6.395





Abstract

This study presents a method for the quantitative analysis of residual vinyl chloride monomer (VCM)in PVC products. In elution solvent, the extraction efficiency was similar by ethanol, THF, and acetone, but using n-hexane, it indicated relatively low extraction efficiency. Measuring VCM in the pulverized PVC samples, it showed reasonable results in both the direct injection method and headspace method with GC/MS. Regarding analysis of VCM in the intermediate sponge samples, five laboratories showed good results, and from the results, it was considered that VCM quantitative method in this study was reliable.

keywords
vinyl chloride monomer, polyvinyl chloride, plastics, test method

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