A Study on the Precursor of $BaTiO_3$ Synthesized in Water
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1992, v.5 no.4, pp.409-415
Kim, Seungwon
Huh, Woo Young
Lee, Chul
Kim,
S., Huh,
W. Y., &
Lee,
C.
(1992). A Study on the Precursor of <TEX>$BaTiO_3$</TEX> Synthesized in Water. , 5(4), 409-415.
Abstract
Factor analysis was applied to X-ray diffraction patterns of the precursor of $BaTiO_3$. For that purpose, the precursor was synthesized in water solvent system using $Ba(NO_3)_2$ and $TiO(NO_3)_2$ as the starting materials and calcined at various temperatures. The samples obtained from the various calcined temperatures were analyzed by the X-ray diffractometer. Factor analysis was applied to the intensity data of the X-ray diffraction patterns. As the results, three factors were found and they were found to be $BaCO_3$, $BaTiO_3$ and $Ba_2TiO_4$. The relative concentrations of the three components were estimated during calcination.
- keywords
-
<TEX>$BaTiO_3$</TEX>,
factor analysis,
X-ray diffraction patterns